Technology Process of C26H29BO4
There total 3 articles about C26H29BO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine;
In
1,4-dioxane;
at 110 ℃;
for 3h;
Inert atmosphere;
DOI:10.1039/c3cc42777c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
2: potassium carbonate; potassium iodide / acetone / 12 h / Inert atmosphere; Reflux
3: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine / 1,4-dioxane / 3 h / 110 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); boron tribromide; potassium carbonate; triethylamine; potassium iodide;
In
1,4-dioxane; dichloromethane; acetone;
DOI:10.1039/c3cc42777c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; potassium iodide / acetone / 12 h / Inert atmosphere; Reflux
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine / 1,4-dioxane / 3 h / 110 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); potassium carbonate; triethylamine; potassium iodide;
In
1,4-dioxane; acetone;
DOI:10.1039/c3cc42777c
