1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Base Information

Chemical Name:1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole
CAS No.:135098-43-0
Molecular Formula:C₂₈H₂₈N₂O₄
Molecular Weight:456.541
Hs Code.:

Synonyms:1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Suppliers and Price of 1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

There total 3 articles about 1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 174583-27-8
2-(1-Benzyl-4,5-diphenyl-1H-imidazol-2-yl)-[1,3]dioxane-5,5-dicarboxylic acid diethyl ester

: 135098-43-0
1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1021/jm9505876

Reference yield:

: 20605-01-0
diethyl bis(hydroxymethyl)malonate

: 135098-43-0
1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / pyridinium p-toluenesulfonate / 36 h / Heating

2: 73 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; In tetrahydrofuran;
DOI:10.1021/jm9505876

Reference yield:

: 135098-44-1
1-benzyl-4,5-diphenylimidazole-2-carboxaldehyde

: 135098-43-0
1-benzyl-2-<5,5-bis(ethoxycarbonyl)-1,3-dioxan-2-yl>-4,5-diphenylimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / pyridinium p-toluenesulfonate / 36 h / Heating

2: 73 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; In tetrahydrofuran;
DOI:10.1021/jm9505876