O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

Base Information

Chemical Name:O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine
CAS No.:1278561-63-9
Molecular Formula:C₁₉H₁₈F₃NO₃
Molecular Weight:365.352
Hs Code.:

Synonyms:O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

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Chemical Property of O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

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Technology Process of O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

There total 3 articles about O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1278561-49-1
(E)-4-(trifluoromethyl)benzaldehyde O-4-methoxybenzoyl oxime

: 106-95-6
allyl bromide

: 1278561-63-9
O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2011.01.032

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1278561-63-9
O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: ammonium chloride; zinc / tetrahydrofuran; water

With ammonium chloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2011.01.032

Reference yield:

: 66046-34-2
4-(trifluoromethyl)benzaldehyde oxime

: 1278561-63-9
O-(4-methoxybenzoyl)-N-(1-(4-(trifluoromethyl)phenyl)but-3-enyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: ammonium chloride; zinc / tetrahydrofuran; water

With ammonium chloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2011.01.032