erythro-3-(p-hydroxyphenyl)-4-hexane

Base Information

Chemical Name:erythro-3-(p-hydroxyphenyl)-4-hexane
CAS No.:76412-12-9
Molecular Formula:C₂₁H₂₈O₂
Molecular Weight:312.452
Hs Code.:

erythro-3-(p-hydroxyphenyl)-4-<p-(ethoxymethyl)phenyl>hexane

Synonyms:erythro-3-(p-hydroxyphenyl)-4-hexane

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Chemical Property of erythro-3-(p-hydroxyphenyl)-4-hexane

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Technology Process of erythro-3-(p-hydroxyphenyl)-4-hexane

There total 7 articles about erythro-3-(p-hydroxyphenyl)-4-hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 64-17-5
ethanol

: 39952-71-1
erythro-3-(p-hydroxyphenyl)-4-hexane

: 76412-12-9
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: With hydrogen iodide; for 9h; Heating;
DOI:10.1021/jm00136a013

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 76412-12-9
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 90 percent / pyridine / Ambient temperature

3: 59 percent / AlCl₃ / CH₂Cl₂ / 3 h / 0 °C

4: 87 percent / LiAlH₄ / tetrahydrofuran / 0 °C

5: 82 percent / 48percent aq. hydroiodic acid / 9 h / Heating

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; hydrogen iodide; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00136a013

Reference yield:

: 3929-22-4,5776-73-8,5776-74-9
deoxyhexestrol

: 76412-12-9
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / Ambient temperature

2: 59 percent / AlCl₃ / CH₂Cl₂ / 3 h / 0 °C

3: 87 percent / LiAlH₄ / tetrahydrofuran / 0 °C

4: 82 percent / 48percent aq. hydroiodic acid / 9 h / Heating

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; hydrogen iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00136a013