methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

Base Information

Chemical Name:methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate
CAS No.:959992-65-5
Molecular Formula:C₁₈H₂₃N₃O₃
Molecular Weight:329.399
Hs Code.:

Synonyms:methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

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Chemical Property of methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

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Technology Process of methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

There total 1 articles about methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 959992-66-6
methyl N-(tert-butoxycarbonyl)-4-[({6-[(tert-butoxycarbonyl)(methyl)amino]pyridin-2-yl}methoxy)methyl]-L-phenylalaninate

: 959992-65-5
methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

Guidance literature:: methyl N-(tert-butoxycarbonyl)-4-[({6-[(tert-butoxycarbonyl)(methyl)amino]pyridin-2-yl}methoxy)methyl]-L-phenylalaninate; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With ammonia; In methanol; dichloromethane;

Reference yield:

: 959992-65-5
methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: C₂₅H₂₅Cl₂N₃O₄

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 959992-65-5
methyl 4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalaninate

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: N-[(2,6-dichlorophenyl)carbonyl]-4-({[6-(methylamino)pyridin-2-yl]methoxy}methyl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: lithium hydroxide; water / dichloromethane / 2 h

With lithium hydroxide; water; triethylamine; In dichloromethane;