rac-2-(p-tolyl)-2,3-dihydrofuran

Base Information

Chemical Name:rac-2-(p-tolyl)-2,3-dihydrofuran
CAS No.:123710-52-1
Molecular Formula:C₁₁H₁₂O
Molecular Weight:160.216
Hs Code.:

Synonyms:rac-2-(p-tolyl)-2,3-dihydrofuran

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Chemical Property of rac-2-(p-tolyl)-2,3-dihydrofuran

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Technology Process of rac-2-(p-tolyl)-2,3-dihydrofuran

There total 13 articles about rac-2-(p-tolyl)-2,3-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 127559-52-8
1-(p-tolyl)buta-2,3-dien-1-ol

: 123710-52-1
rac-2-(p-tolyl)-2,3-dihydrofuran

Guidance literature:: With trimethylamine-N-oxide; tricarbonyl(η⁴-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron; potassium carbonate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/acscatal.7b03515

Reference yield: 85.0%

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 624-31-7
4-tolyl iodide

: 123710-52-1
rac-2-(p-tolyl)-2,3-dihydrofuran

Guidance literature:: With trans-di(μ-acetato)-bis[o-(di-o-tolylphosphino)benzyl]-dipalladium(II); sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 120 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.1c04120

Reference yield: 55.0%

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 106-38-7
para-bromotoluene

: 123710-52-1
rac-2-(p-tolyl)-2,3-dihydrofuran

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2′-(dicyclohexylphophanyl)-N₂,N₂,N₆,N₆-tetramethyl[1,1′-biphenyl]-2,6-diamine; N-Methyldicyclohexylamine; In 1,4-dioxane; at 110 ℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.6b02158