6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Base Information

Chemical Name:6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene
CAS No.:1260249-07-7
Molecular Formula:C₃₈H₂₈N₂
Molecular Weight:512.654
Hs Code.:

Synonyms:6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

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Chemical Property of 6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Chemical Property:

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Technology Process of 6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

There total 4 articles about 6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260228-95-2
12,12-dimethyl-11,12-dihydroindeno[2,1-a]carbazole

: 1260248-98-3
6-(2,6-dibromopyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

: 497-19-8
sodium carbonate

: 175422-04-5
2,6-dibromo-4-nitropyridine

: 98-80-6
phenylboronic acid

: 1260249-07-7
6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: With NaH; Pd(PPh₃)4; In N-methyl-acetamide; 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 577-19-5
2-nitrophenyl bromide

: 1260249-07-7
6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate / toluene; 1,4-dioxane; ethanol; water

2: triethyl phosphite

3: NaH / Pd(PPh₃)4 / N,N-dimethyl-formamide; 1,2-dimethoxyethane; mineral oil; N-methyl-acetamide

With NaH; triethyl phosphite; Pd(PPh₃)4; palladium diacetate; In 1,4-dioxane; N-methyl-acetamide; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 333432-28-3
9,9-dimethyl-9H-fluoren-2-yl-2-boronic acid

: 1260249-07-7
6-(2,6-Diphenylpyridin-4-yl)-12,12-dimethyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate / toluene; 1,4-dioxane; ethanol; water

2: triethyl phosphite

3: NaH / Pd(PPh₃)4 / N,N-dimethyl-formamide; 1,2-dimethoxyethane; mineral oil; N-methyl-acetamide

With NaH; triethyl phosphite; Pd(PPh₃)4; palladium diacetate; In 1,4-dioxane; N-methyl-acetamide; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; toluene; mineral oil;