(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

Base Information

Chemical Name:(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine
CAS No.:1312017-24-5
Molecular Formula:C₂₄H₃₁N₃O₂S
Molecular Weight:425.595
Hs Code.:

Synonyms:(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

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Chemical Property of (2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

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Technology Process of (2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

There total 13 articles about (2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1312019-77-4
2-[2-cyclopentyl-1-(4-ethenesulfonyl-phenyl)-ethyl]-1H-pyrrolo[2,3-b]pyridine

: 124-40-3
dimethyl amine

: 1312017-24-5
(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

Guidance literature:: In methanol; at 25 ℃; for 0.333333h;

Reference yield:

: 237429-33-3
4-mercaptophenylboronic acid

: 1312017-24-5
(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 7 h / 25 °C

2.1: sodium periodate / water; methanol / 16 h / 25 °C

2.2: 2 h / 25 °C

3.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane; water / 2 h / 100 °C / Microwave irradiation

4.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 5 h / 50 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 50 °C / 2585.81 Torr

6.1: boron tribromide / dichloromethane / 1 h / 0 °C

7.1: triethylamine / dichloromethane / 0.5 h / 0 °C

8.1: methanol / 0.33 h / 25 °C

With sodium periodate; water; hydrogen; boron tribromide; sodium carbonate; potassium carbonate; triethylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1032825-12-9
(4-{[2-(methoxy)ethyl]thio}phenyl)boronic acid

: 1312017-24-5
(2-{4-[2-cyclopentyl-1-(1H-pyrrolo[2,3-b]pyridin-2-yl)-ethyl]-benzenesulfonyl}-ethyl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium periodate / water; methanol / 16 h / 25 °C

1.2: 2 h / 25 °C

2.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane; water / 2 h / 100 °C / Microwave irradiation

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 5 h / 50 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 50 °C / 2585.81 Torr

5.1: boron tribromide / dichloromethane / 1 h / 0 °C

6.1: triethylamine / dichloromethane / 0.5 h / 0 °C

7.1: methanol / 0.33 h / 25 °C

With sodium periodate; water; hydrogen; boron tribromide; sodium carbonate; triethylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water;