1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

Base Information

Chemical Name:1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol
CAS No.:124077-36-7
Molecular Formula:C₃₆H₄₆O₁₀
Molecular Weight:638.755
Hs Code.:

Synonyms:1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

Chemical Property:

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Technology Process of 1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

There total 6 articles about 1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 117325-96-9
2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribitol

: 53402-29-2
2,3,5-tri-O-acetyl-β-D-ribofuranosyl chloride

: 124077-36-7
1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

Guidance literature:: With 4 A molecular sieve; silver perchlorate; In acetonitrile; at -40 ℃;
DOI:10.1016/S0040-4039(00)80342-1

Reference yield: 97.0%

: 117325-96-9
2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribitol

: 39925-22-9
2,3,5-Tris-O-acetyl-β-D-ribofuranosyl bromide

: 124077-36-7
1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

Guidance literature:: With 4 A molecular sieve; silver perchlorate; In acetonitrile; at -40 ℃;
DOI:10.1016/S0040-4039(00)80342-1

Reference yield:

: 117325-94-7
5-O-[(4-Methoxyphenyl)diphenylmethyl]-2,3,4-tris-O-(phenylmethyl)-D-ribose-diethyldithioacetal

: 124077-36-7
1-O-β-D-Ribofuranosyl-5-O-(trimethylacetyl)-2,3,4-tris-O-(phenylmethyl)-D-ribitol

Guidance literature:: Multi-step reaction with 4 steps

1: p-toluenesulfonic acid / methanol

2: 98 percent / pyridine / DMAP / CH₂Cl₂ / Ambient temperature

3: 1.) HgCl₂, CdCO₃, 2.) NaBH₃CN, further reducing agent and solvent / 1.) acetone-water, 2.) dimethoxyethane

4: 97 percent / silver perchlorate, 4-Angstroem molecular sieves / acetonitrile / -40 °C

With pyridine; cadmium(II) carbonate; 4 A molecular sieve; silver perchlorate; sodium cyanoborohydride; toluene-4-sulfonic acid; mercury dichloride; dmap; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)80342-1