2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Base Information

Chemical Name:2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal
CAS No.:117325-95-8
Molecular Formula:C₃₅H₄₆O₅S₂
Molecular Weight:610.879
Hs Code.:

Synonyms:2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Suppliers and Price of 2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

There total 6 articles about 2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3282-30-2
pivaloyl chloride

: 108713-89-9
(2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentan-1-ol

: 117325-95-8
2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Guidance literature:: With pyridine; dmap; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(00)80342-1

Reference yield:

: 7152-47-8
D-ribose diethyl dithioacetal

: 117325-95-8
2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / silver nitrate / tetrahydrofuran

2: sodium hydride / dimethylformamide

3: p-toluenesulfonic acid / methanol

4: 98 percent / pyridine / DMAP / CH₂Cl₂ / Ambient temperature

With pyridine; sodium hydride; toluene-4-sulfonic acid; silver nitrate; dmap; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)80342-1

Reference yield:

: 100-39-0
benzyl bromide

: 117325-95-8
2,3,4-Tris-O-(phenylmethyl)-5-O-(trimethylacetyl)-D-ribose diethyldithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethylformamide

2: p-toluenesulfonic acid / methanol

3: 98 percent / pyridine / DMAP / CH₂Cl₂ / Ambient temperature

With pyridine; sodium hydride; toluene-4-sulfonic acid; dmap; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)80342-1