methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside
CAS No.:1012044-74-4
Molecular Formula:C₂₅H₃₀O₉
Molecular Weight:474.508
Hs Code.:

Synonyms:methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

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Technology Process of methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

There total 1 articles about methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-30-5
succinic acid anhydride

: 58341-67-6
methyl 2,4-di-O-benzyl-α-D-glucopyranoside

: 1012044-74-4
methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 20 ℃; for 16h;
DOI:10.1021/jo701902f

Reference yield: 98.0%

: 1012044-74-4
methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

: 635727-37-6
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

: 1012044-80-2
methyl 2,4-di-O-benzyl-3-O-(β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside; With TentaGel amine resin; dicyclohexyl-carbodiimide; In dichloromethane; for 72h;

2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole; With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 48h;

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 48h; pH=8 - 9; Further stages.;
DOI:10.1021/jo701902f

Reference yield: 98.0%

: 1012044-74-4
methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside

: 744245-92-9
2-thiazolinyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 1012044-80-2
methyl 2,4-di-O-benzyl-3-O-(β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: methyl 2,4-di-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-α-D-glucopyranoside; With dicyclohexyl-carbodiimide; In dichloromethane; for 72h;

2-thiazolinyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; With 3 A molecular sieve; methyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 96h;

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 48h; pH=8 - 9; Further stages.;
DOI:10.1021/jo701902f