2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile

Base Information

• Chemical Name: 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile
• CAS No.: 1596326-80-5
• Molecular Formula: C₁₈H₁₆N₆S
• Molecular Weight: 348.431

Synonyms:2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile

Chemical Property of 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile

There total 2 articles about 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

aniline hydrochloride (142-04-1,36663-09-9) + 3-ethylthio-5-cyanomethyl-4-phenyl-1,2,4-triazole (223589-66-0) → 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile (1596326-80-5)

Guidance literature:

aniline hydrochloride; With sodium nitrite; In water;

3-ethylthio-5-cyanomethyl-4-phenyl-1,2,4-triazole; With sodium acetate; In ethanol; at 20 ℃; for 24h;

DOI:10.3390/molecules19032993

Reference yield:

benzene diazonium chloride (100-34-5) + 3-ethylthio-5-cyanomethyl-4-phenyl-1,2,4-triazole (223589-66-0) → 2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile (1596326-80-5)

Guidance literature:

With sodium acetate; In ethanol; water;

DOI:10.1002/jhet.2363

Reference yield: 75.0%

2-(5-ethylthio-4-phenyl-4H-[1,2,4-]-triazol-3-yl)-2-(phenylhydrazono)acetonitrile (1596326-80-5) + para-bromophenacyl bromide (99-73-0,132309-76-3) → (4-amino-3-(5-ethylthio-4-phenyl-4H-1,2,4-triazol-3-yl)-1-phenyl-1H-pyrazol-5-yl)(4-bromophenyl)methanone

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 80 ℃;

DOI:10.1002/jhet.2363

upstream raw materials:

aniline hydrochloride

3-ethylthio-5-cyanomethyl-4-phenyl-1,2,4-triazole

benzene diazonium chloride

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