4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

Base Information

Chemical Name:4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole
CAS No.:162687-93-6
Molecular Formula:C₂₇H₃₈N₄S
Molecular Weight:450.692
Hs Code.:

4,5-diphenyl-2-<<2-<N-methyl-N-<2-(N-heptylamino)ethyl>amino>ethyl>thio>-1H-imidazole

Synonyms:4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

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Chemical Property of 4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

Chemical Property:

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Technology Process of 4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

There total 9 articles about 4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162687-92-5
2-(4,5-Diphenyl-1H-imidazol-2-ylsulfanyl)-N-heptylcarbamoylmethyl-N-methyl-acetamide

: 162687-93-6
4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; for 15h; Yield given; Heating;
DOI:10.1021/jm00007a004

Reference yield:

: 111-68-2
1-Heptylamine

: 162687-93-6
4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / toluene / 18 h / Heating

2: 85 percent / LiAlH₄ / tetrahydrofuran / 18 h / Heating

3: 1.) 1-hydroxybenzotriazole hydrate, 2.) dicyclohexylcarbodiimide / 1.) DMF, RT, 20 min, 2.) DMF, RT, 48 h

4: sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 15 h / Heating

With lithium aluminium tetrahydride; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene;
DOI:10.1021/jm00007a004

Reference yield:

: 65332-01-6
methyl N-(2-chloroacetyl)glycine

: 162687-93-6
4,5-diphenyl-2-<<2-amino>ethyl>thio>-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / K₂CO₃ / tetrahydrofuran / 14 h / Heating

2: 1.) 1-hydroxybenzotriazole hydrate, 2.) dicyclohexylcarbodiimide / 1.) DMF, RT, 20 min, 2.) DMF, RT, 48 h

3: sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 15 h / Heating

With potassium carbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene;
DOI:10.1021/jm00007a004