C₃₃H₄₇ClN₄O₃S

Base Information

Chemical Name:C₃₃H₄₇ClN₄O₃S
CAS No.:1308662-31-8
Molecular Formula:C₃₃H₄₇ClN₄O₃S
Molecular Weight:615.28
Hs Code.:

C<sub>33</sub>H<sub>47</sub>ClN<sub>4</sub>O<sub>3</sub>S

Synonyms:C₃₃H₄₇ClN₄O₃S

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Chemical Property of C₃₃H₄₇ClN₄O₃S

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Technology Process of C₃₃H₄₇ClN₄O₃S

There total 8 articles about C₃₃H₄₇ClN₄O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1308662-30-7
C₂₃H₃₀ClN₃O₄S

: 13293-47-5
(1S,2S,3S,5R)-(+)-isopinocampheylamine

: 1308662-31-8
C₃₃H₄₇ClN₄O₃S

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h; Inert atmosphere;

Reference yield:

: 82072-23-9
3-(bromomethyl)benzaldehyde

: 1308662-31-8
C₃₃H₄₇ClN₄O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / dichloromethane; N,N-dimethyl-formamide / 20 h / 20 °C

2.1: triethylamine / methanol / 0.17 h

2.2: 0.25 h / 20 °C / Inert atmosphere

2.3: 20 °C / Inert atmosphere; Cooling with ice

3.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 2 h / 20 °C

3.2: pH 4.5

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; benzotriazol-1-ol; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 28188-41-2
m-(bromomethyl)benzonitrile

: 1308662-31-8
C₃₃H₄₇ClN₄O₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / chlorobenzene; chloroform / 1 h / 5 °C / Cooling with ice

2.1: caesium carbonate / dichloromethane; N,N-dimethyl-formamide / 20 h / 20 °C

3.1: triethylamine / methanol / 0.17 h

3.2: 0.25 h / 20 °C / Inert atmosphere

3.3: 20 °C / Inert atmosphere; Cooling with ice

4.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 2 h / 20 °C

4.2: pH 4.5

5.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; diisobutylaluminium hydride; benzotriazol-1-ol; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; chlorobenzene;