C₃₂H₃₀Cl₂N₂O₂S

Base Information

Chemical Name:C₃₂H₃₀Cl₂N₂O₂S
CAS No.:1437869-88-9
Molecular Formula:C₃₂H₃₀Cl₂N₂O₂S
Molecular Weight:577.574
Hs Code.:

C<sub>32</sub>H<sub>30</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₃₂H₃₀Cl₂N₂O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₀Cl₂N₂O₂S

Chemical Property:

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Technology Process of C₃₂H₃₀Cl₂N₂O₂S

There total 7 articles about C₃₂H₃₀Cl₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 110-91-8,99108-56-2
morpholine

: 1437869-85-6
C₂₅H₁₇Cl₂NOS

: 109-70-6
1.3-chlorobromopropane

: 1437869-88-9
C₃₂H₃₀Cl₂N₂O₂S

Guidance literature:: C₂₅H₁₇Cl₂NOS; With potassium carbonate; In N,N-dimethyl-formamide; for 0.5h;

1.3-chlorobromopropane; In N,N-dimethyl-formamide; at 80 ℃; for 0.75h;

morpholine; With triethylamine; In 1,4-dioxane; for 24h; Reflux;
DOI:10.1016/j.bmc.2013.03.070

Reference yield:

: 1878-66-6
4-chlorophenylacetic Acid

: 1437869-88-9
C₃₂H₃₀Cl₂N₂O₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride / dichloromethane / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 20 °C

3.1: titanium tetrachloride; pyridine / tetrahydrofuran / 0 - 20 °C

4.1: sulfur; diethylamine / tetrahydrofuran / 20 °C

5.1: sodium hydroxide; water / ethanol / Reflux

6.1: acetic acid / 2 h / Reflux

7.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

7.2: 0.75 h / 80 °C

7.3: 24 h / Reflux

With pyridine; aluminum (III) chloride; oxalyl dichloride; water; titanium tetrachloride; potassium carbonate; sulfur; acetic acid; diethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 2.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmc.2013.03.070

Reference yield:

: 51490-05-2
1,2-bis(4-chlorophenyl)ethanone

: 1437869-88-9
C₃₂H₃₀Cl₂N₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: titanium tetrachloride; pyridine / tetrahydrofuran / 0 - 20 °C

2.1: sulfur; diethylamine / tetrahydrofuran / 20 °C

3.1: sodium hydroxide; water / ethanol / Reflux

4.1: acetic acid / 2 h / Reflux

5.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

5.2: 0.75 h / 80 °C

5.3: 24 h / Reflux

With pyridine; water; titanium tetrachloride; potassium carbonate; sulfur; acetic acid; diethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.03.070