(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Base Information

Chemical Name:(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)
CAS No.:1519044-32-6
Molecular Formula:C₂₄H₃₇IO₃Si₂
Molecular Weight:556.631
Hs Code.:

Synonyms:(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Suppliers and Price of (4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

There total 6 articles about (4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1519044-31-5
2-(3,4-dihydroxyphenoxy)iodobenzene

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1519044-32-6
(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1,2-dimethoxy-4-(2-nitrophenoxy)benzene

: 1519044-32-6
(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate; palladium 10% on activated carbon / ethanol / 5 h / 20 °C

2.1: sulfuric acid; sodium nitrite / water / 1 h / 0 - 5 °C

2.2: 4.5 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 6 h / 20 °C

4.1: 1H-imidazole; dmap / dichloromethane / 3 h / 20 °C

With 1H-imidazole; dmap; sulfuric acid; palladium 10% on activated carbon; boron tribromide; hydrazine hydrate; sodium nitrite; In ethanol; dichloromethane; water;
DOI:10.1002/cmdc.201400058

Reference yield:

: 640766-60-5
2-(3,4-dimethoxyphenoxy)aniline

: 1519044-32-6
(4-(2-iodophenoxy)-1,2-phenylene)bis(oxy)bis(tert-butyldimethylsilane)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / water / 1 h / 0 - 5 °C

1.2: 4.5 h / 0 - 20 °C

2.1: boron tribromide / dichloromethane / 6 h / 20 °C

3.1: 1H-imidazole; dmap / dichloromethane / 3 h / 20 °C

With 1H-imidazole; dmap; sulfuric acid; boron tribromide; sodium nitrite; In dichloromethane; water;
DOI:10.1002/cmdc.201400058