Technology Process of C13H17NO4S
There total 3 articles about C13H17NO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-[1-(2-oxoethyl)allyl]-4-methylbenzenesulfonamide; (methoxymethyl)triphenylphosphonium chloride;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
N-[1-(2-oxoethyl)allyl]-4-methylbenzenesulfonamide;
In
tetrahydrofuran;
at -78 ℃;
for 2h;
With
jones reagent;
In
acetone;
at 20 ℃;
for 0.333333h;
Further stages.;
DOI:10.3987/COM-06-10837
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 89 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 20 °C
2.1: 82 percent / pyridinium chlorochromate; Celite / CH2Cl2 / 20 h / 20 °C
3.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C
3.2: tetrahydrofuran / 2 h / -78 °C
3.3: 68 percent / Jones reagent / acetone / 0.33 h / 20 °C
With
lithium aluminium tetrahydride; n-butyllithium; Celite; pyridinium chlorochromate;
In
tetrahydrofuran; hexane; dichloromethane;
3.1: Wittig olefination / 3.3: Jones oxidation;
DOI:10.3987/COM-06-10837
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 82 percent / pyridinium chlorochromate; Celite / CH2Cl2 / 20 h / 20 °C
2.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: tetrahydrofuran / 2 h / -78 °C
2.3: 68 percent / Jones reagent / acetone / 0.33 h / 20 °C
With
n-butyllithium; Celite; pyridinium chlorochromate;
In
tetrahydrofuran; hexane; dichloromethane;
2.1: Wittig olefination / 2.3: Jones oxidation;
DOI:10.3987/COM-06-10837
![N-[1-(2-oxoethyl)allyl]-4-methylbenzenesulfonamide](/Databaselist/images/loading.webp)
