3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

Base Information

Chemical Name:3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate
CAS No.:135573-94-3
Molecular Formula:C₂₈H₃₄O₅
Molecular Weight:450.575
Hs Code.:

Synonyms:3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

Suppliers and Price of 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

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Technology Process of 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

There total 3 articles about 3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83205-52-1,2080-86-6
3β-benzoyloxy-androst-5-en-17-one

: 135573-94-3
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. sodium hydrogen phosphate, aq. peroxyacetic acid / CHCl₃ / 2 h

2: 87 percent / 72percent aq. perchloric acid / dioxane; acetone / 3 h

3: 2.) H₂SO₄ / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h

With peracetic acid; disodium hydrogenphosphate; perchloric acid; sulfuric acid; In 1,4-dioxane; chloroform; acetone;

Reference yield:

: Benzoic acid (3S,8R,9S,10R,13S,14S)-10,13-dimethyl-17-oxo-hexadecahydro-20-oxa-cyclopropa[5,6]cyclopenta[a]phenanthren-3-yl ester

: 135573-94-3
3β,6β-dihydroxy-5-methyl-19-nor-5β-androst-9-en-17-one 3-benzoate 6-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 72percent aq. perchloric acid / dioxane; acetone / 3 h

2: 2.) H₂SO₄ / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h

With perchloric acid; sulfuric acid; In 1,4-dioxane; acetone;