1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Base Information

Chemical Name:1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester
CAS No.:1298046-05-5
Molecular Formula:C₁₉H₂₅NO₆
Molecular Weight:363.411
Hs Code.:

Synonyms:1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

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Chemical Property of 1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Chemical Property:

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Technology Process of 1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

There total 2 articles about 1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60444-56-6
3-acetoxy-4-methoxybenzoic acid

: 92398-50-0
methyl 1-amino-cycloheptanecarboxylate hydrochloride

: 1298046-05-5
1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: With O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 645-08-9,74309-78-7
Isovanillic acid

: 1298046-05-5
1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3 h / 140 °C / Inert atmosphere

1.2: 1 h / 100 °C / Inert atmosphere; Reflux

2.1: N-ethyl-N,N-diisopropylamine; O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1298046-05-5
1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

: 1298047-78-5
1-(3-hydroxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: 1-(3-acetoxy-4-methoxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester; With potassium carbonate; In methanol; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In methanol; water; Inert atmosphere;