N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

Base Information

Chemical Name:N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide
CAS No.:144582-33-2
Molecular Formula:C₃₂H₄₃N₃O₃
Molecular Weight:517.712
Hs Code.:

Synonyms:N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

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Chemical Property of N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

Chemical Property:

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Technology Process of N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

There total 18 articles about N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19417-59-5
1,4-bis-(3-bromopropyl)-benzene

: 144582-33-2
N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 13 steps

1: 1) NaOEt, 2) aq. KOH / 1) EtOH

2: dimethylformamide / Heating

3: TsOH / toluene

4: NaNO₂, CF₃CO₂H

5: aq. KOH

6: SOCl₂ / Heating

7: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

8: B₂H₆ / tetrahydrofuran

9: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

10: PhCH₂ONa / 100 °C / 12 Torr

11: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

12: dimethylformamide / Heating

13: POCl₃ / CH₂Cl₂

With potassium hydroxide; thionyl chloride; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 19417-58-4
[1,4-phenylene]-bis(3-hydroxypropane)

: 144582-33-2
N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 14 steps

1: HBr

2: 1) NaOEt, 2) aq. KOH / 1) EtOH

3: dimethylformamide / Heating

4: TsOH / toluene

5: NaNO₂, CF₃CO₂H

6: aq. KOH

7: SOCl₂ / Heating

8: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

9: B₂H₆ / tetrahydrofuran

10: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

11: PhCH₂ONa / 100 °C / 12 Torr

12: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

13: dimethylformamide / Heating

14: POCl₃ / CH₂Cl₂

With potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 4251-21-2
3,3'-(1,4-phenylene)dipropanoic acid

: 144582-33-2
N-{2,5-Bis-[5-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)-pentyl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 16 steps

1: 1) SOCl₂, 2) NEt₃

2: B₂H₆

3: HBr

4: 1) NaOEt, 2) aq. KOH / 1) EtOH

5: dimethylformamide / Heating

6: TsOH / toluene

7: NaNO₂, CF₃CO₂H

8: aq. KOH

9: SOCl₂ / Heating

10: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

11: B₂H₆ / tetrahydrofuran

12: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

13: PhCH₂ONa / 100 °C / 12 Torr

14: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

15: dimethylformamide / Heating

16: POCl₃ / CH₂Cl₂

With potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; triethylamine; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;