[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane

Base Information

• Chemical Name: [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane
• CAS No.: 170961-27-0
• Molecular Formula: C₃₄H₇₈Br₂GeSi₈
• Molecular Weight: 944.075

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane

Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane

Chemical Property:

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane

There total 2 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-Bromosuccinimide (128-08-5) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germane → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane (170961-27-0)

Guidance literature:

In benzene; room temp., stirring (10 h); chromatography (SiO2, benzene), dissolving (CH2Cl2), addition (ethanol),evaporation (room temp., reduced pressure); elem. anal;

DOI:10.1021/ja991147x

Reference yield:

1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene (115160-05-9) → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane (170961-27-0) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dichlorogermane + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]bromochlorogermane

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

In tetrahydrofuran;

DOI:10.1021/ja991147x

Reference yield: 55.0%

lithium aluminium tetrahydride (16853-85-3) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dibromogermane (170961-27-0) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]dichlorogermane + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]bromochlorogermane → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germane

Guidance literature:

In tetrahydrofuran; 0°C, warming (room temp.), refluxing (10 h); extraction, drying, dissolving (CH2Cl2), addition (ethanol),evaporation (room temp.,reduced pressure); elem. anal;

DOI:10.1021/ja991147x

upstream raw materials:

N-Bromosuccinimide

1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

Downstream raw materials:

[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germylene

GeS₄(CH(Si(CH₃)3)2)(C₆H₂(CH(Si(CH₃)3)2)3)

[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germaneselone

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