ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

Base Information

Chemical Name:ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate
CAS No.:1228186-98-8
Molecular Formula:C₁₄H₂₃NO₅
Molecular Weight:285.34
Hs Code.:

Synonyms:ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

Chemical Property:

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Technology Process of ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

There total 6 articles about ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1334880-42-0
tert-butyl (1R,2S,5S)-7-oxo-6-oxabicyclo[3.2.1]oct-3-en-2-ylcarbamate

: 141-52-6
sodium ethanolate

: 1228186-98-8
ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

Guidance literature:: In ethanol; at -10 ℃; for 1h;
DOI:10.1016/j.tet.2012.09.085

Reference yield: 70.0%

: 1334880-42-0
tert-butyl (1R,2S,5S)-7-oxo-6-oxabicyclo[3.2.1]oct-3-en-2-ylcarbamate

: 1228186-98-8
ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

Guidance literature:: With ethanol; sodium ethanolate; at 0 ℃; for 1h;
DOI:10.1002/ejoc.201100583

Reference yield:

: ethyl rac-(1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

: 1228186-98-8
ethyl (1R,2S,5S)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

: ethyl (1S,2R,5R)-2-(tert-butoxycarbonylamino)-5-hydroxycyclohex-3-enecarboxylate

: C₁₂H₁₉NO₅

Guidance literature:: With resin-supported recombinant Candida antarctica lipase B; water; In tert-butyl methyl ether; at 60 ℃; for 240h; optical yield given as %ee; enantioselective reaction; Enzymatic reaction;
DOI:10.3390/molecules15063998