o-cyanobenzyl isothiocyanate

Base Information

• Chemical Name: o-cyanobenzyl isothiocyanate
• CAS No.: 145083-86-9
• Molecular Formula: C₉H₆N₂S
• Molecular Weight: 174.226

Synonyms:o-cyanobenzyl isothiocyanate

Chemical Property of o-cyanobenzyl isothiocyanate

Chemical Property:

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Technology Process of o-cyanobenzyl isothiocyanate

There total 1 articles about o-cyanobenzyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

potassium thioacyanate (333-20-0) + 2-(bromomethyl)benzonitrile (22115-41-9) → o-cyanobenzyl isothiocyanate (145083-86-9)

Guidance literature:

With sodium iodide; In N,N-dimethyl-formamide; at 90 ℃; for 9h;

DOI:10.1016/S0040-4020(01)90364-3

Reference yield: 90.0%

o-cyanobenzyl isothiocyanate (145083-86-9) → o-cyanobenzylthiosemicarbazide (145083-87-0)

Guidance literature:

With hydrazine hydrate; In ethanol; for 0.25h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90364-3

upstream raw materials:

potassium thioacyanate

2-(bromomethyl)benzonitrile

Downstream raw materials:

o-cyanobenzylthiosemicarbazide

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