(2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate

Base Information

• Chemical Name: (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate
• CAS No.: 1226896-63-4
• Molecular Formula: C₃₄H₄₁IN₂O₈
• Molecular Weight: 732.613

Synonyms:(2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate

Chemical Property of (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate

Chemical Property:

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Technology Process of (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate

There total 7 articles about (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ³-iodanediyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(2R,2'R)-2,2'-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide) (1226896-38-3) + acetic acid (64-19-7,77671-22-8) → (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ3-iodanediyl diacetate (1226896-63-4)

Guidance literature:

With Selectfluor; In acetonitrile; for 5h; Inert atmosphere;

DOI:10.1002/chem.201603022

Reference yield:

2-iodoresorcinol (41046-67-7) → (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ3-iodanediyl diacetate (1226896-63-4)

Guidance literature:

Multi-step reaction with 5 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Darkness

2.1: Selectfluor / acetonitrile / 5 h / Inert atmosphere

3.1: sodium hydroxide / tetrahydrofuran; methanol / 0 - 20 °C

4.1: thionyl chloride / 1.5 h / Reflux

4.2: 0 - 20 °C / Inert atmosphere

5.1: Selectfluor / acetonitrile / 5 h / Inert atmosphere

With thionyl chloride; di-isopropyl azodicarboxylate; Selectfluor; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; acetonitrile;

DOI:10.1002/chem.201603022

Reference yield:

(2R,2'R)-dimethyl 2,2'-((2-iodo-1,3-phenylene)bis(oxy))dipropanoate (1255651-99-0) → (2,6-bis(((R)-1-(mesitylamino)-1-oxopropan-2-yl)oxy)-phenyl)-λ3-iodanediyl diacetate (1226896-63-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: Selectfluor / acetonitrile / 5 h / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; methanol / 0 - 20 °C

3.1: thionyl chloride / 1.5 h / Reflux

3.2: 0 - 20 °C / Inert atmosphere

4.1: Selectfluor / acetonitrile / 5 h / Inert atmosphere

With thionyl chloride; Selectfluor; sodium hydroxide; In tetrahydrofuran; methanol; acetonitrile;

DOI:10.1002/chem.201603022

upstream raw materials:

(2R,2'R)-2,2'-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

acetic acid

2-iodoresorcinol

(2R,2'R)-dimethyl 2,2'-((2-iodo-1,3-phenylene)bis(oxy))dipropanoate

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