Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

Base Information

Chemical Name:Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester
CAS No.:124832-38-8
Molecular Formula:C₁₉H₂₆N₂O₇
Molecular Weight:394.425
Hs Code.:

Synonyms:Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

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Chemical Property of Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

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Technology Process of Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

There total 5 articles about Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 124832-37-7
Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

: 124832-38-8
Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 20876-28-2
2-(2-methoxy-6-nitrophenyl)acetic acid

: 124832-38-8
Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1) SOCl₂ / 2) TiCl₄

2: 89 percent / 9-BBN, H₂O₂, NaOH

3: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

4: 94 percent

5: 89 percent / H₂SO₄ / methanol

6: 75 percent / Zn, NH₄Cl / tetrahydrofuran; H₂O

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; thionyl chloride; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; ammonium chloride; dimethyl sulfoxide; triethylamine; zinc; titanium tetrachloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 124832-33-3
1-(2-Methoxy-6-nitro-phenyl)-pent-4-en-2-one

: 124832-38-8
Carbonic acid allyl ester 1-cyano-5-(2-hydroxyamino-6-methoxy-phenyl)-4,4-dimethoxy-pentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / 9-BBN, H₂O₂, NaOH

2: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

3: 94 percent

4: 89 percent / H₂SO₄ / methanol

5: 75 percent / Zn, NH₄Cl / tetrahydrofuran; H₂O

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; ammonium chloride; dimethyl sulfoxide; triethylamine; zinc; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)99254-2