Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Base Information

Chemical Name:Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester
CAS No.:124832-37-7
Molecular Formula:C₁₉H₂₄N₂O₈
Molecular Weight:408.408
Hs Code.:

Synonyms:Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Suppliers and Price of Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

There total 4 articles about Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 124832-36-6
Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

: 149-73-5
trimethyl orthoformate

: 124832-37-7
Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Guidance literature:: With sulfuric acid; In methanol;
DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 20876-28-2
2-(2-methoxy-6-nitrophenyl)acetic acid

: 124832-37-7
Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1) SOCl₂ / 2) TiCl₄

2: 89 percent / 9-BBN, H₂O₂, NaOH

3: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

4: 94 percent

5: 89 percent / H₂SO₄ / methanol

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; thionyl chloride; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; titanium tetrachloride; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 124832-33-3
1-(2-Methoxy-6-nitro-phenyl)-pent-4-en-2-one

: 124832-37-7
Carbonic acid allyl ester 1-cyano-4,4-dimethoxy-5-(2-methoxy-6-nitro-phenyl)-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 9-BBN, H₂O₂, NaOH

2: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

3: 94 percent

4: 89 percent / H₂SO₄ / methanol

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; oxalyl dichloride; sulfuric acid; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)99254-2