14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

Base Information

Chemical Name:14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester
CAS No.:187600-67-5
Molecular Formula:C₂₄H₃₂O₉S
Molecular Weight:496.579
Hs Code.:

Synonyms:14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

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Chemical Property of 14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

Chemical Property:

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Technology Process of 14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

There total 5 articles about 14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-59-9
p-toluenesulfonyl chloride

: 195071-47-7
14-hydroxy-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

: 187600-67-5
14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

Guidance literature:: With pyridine; at -0.16 ℃; for 2h;
DOI:10.1016/j.bmc.2011.05.002

Reference yield:

: 112-60-7
Tetraethylene glycol

: 187600-67-5
14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / BF₃*Et₂O / CH₂Cl₂ / Ambient temperature

2: 69 percent / pyridine / 0 °C

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1039/a606340c

Reference yield:

: 52267-51-3
benzyl diazoacetate

: 187600-67-5
14-[[(4-methylphenyl)sulfonyl]oxy]-3,6,9,12-tetraoxatetradecanoic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / BF₃*Et₂O / CH₂Cl₂ / Ambient temperature

2: 69 percent / pyridine / 0 °C

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1039/a606340c