zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

Base Information

Chemical Name:zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)
CAS No.:102425-07-0
Molecular Formula:C₅₀H₃₉BrN₄OZn
Molecular Weight:857.18
Hs Code.:

Synonyms:zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

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Chemical Property of zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

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Technology Process of zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

There total 4 articles about zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.7%

: 629-03-8
1 ,6-dibromohexane

: 110275-59-7
meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

: 102425-07-0
zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; mixt. of Zn-complex, C6H12Br2 and K2CO3 suspended in dry DMF, stirred for 48 h at room temp.; solvent evapd. under redused pressure, residue dissolved (CHCl3), washed(H2O), org. layer dried (anhyd. Na2SO4), evapd. to remove solvent, resi due purified by chromy. (silica gel, CHCl3), first fraction collected, concd., purifn. repeated twice;
DOI:10.1021/jp0347419

Reference yield:

: 87345-22-0
5-(4'-hydroxyphenyl)-10,15,20-triphenylporphyrin

: 102425-07-0
zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

2: chloroform; methanol / 5 h

With potassium carbonate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1142/S1088424613501101

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 102425-07-0
zinc(II)(5-(4-(ω-bromohexyloxy)phenyl)-10,15,20-triphenylporphyrinate)

Guidance literature:: Multi-step reaction with 3 steps

1: propionic acid / 0.5 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

3: chloroform; methanol / 5 h

With potassium carbonate; In methanol; chloroform; propionic acid; N,N-dimethyl-formamide;
DOI:10.1142/S1088424613501101