Technology Process of C28H36O4Si
There total 1 articles about C28H36O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
N,N-dimethyl-formamide;
for 12h;
Inert atmosphere;
DOI:10.1021/ja906996c
- Guidance literature:
-
With
ammonium cerium (IV) nitrate;
In
water; acetonitrile;
at 0 ℃;
Inert atmosphere;
DOI:10.1021/ja906996c
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / water; acetonitrile / 0.17 h / 0 °C
2.1: 1H-imidazole; dmap / 0 - 20 °C
3.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C
4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C
5.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
5.2: -78 - 20 °C
6.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C
With
1H-imidazole; dmap; n-butyllithium; ammonium cerium (IV) nitrate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/asia.201000882