Technology Process of C20H17NO2
There total 5 articles about C20H17NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyl 3-(6-o-tolylquinolin-3-yl)but-2-enoate;
With
water; lithium hydroxide;
In
tetrahydrofuran;
at 23 ℃;
for 48h;
With
hydrogenchloride;
In
tetrahydrofuran; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine / tetrahydrofuran / 1 h
2: diethyl ether; tetrahydrofuran / 1 h / 0 °C
3: toluene / 1.17 h / 140 - 160 °C / microwave irradiation
4: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 0.33 h / 90 °C / microwave irradiation
5: water; lithium hydroxide / tetrahydrofuran / 48 h / 23 °C
With
4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; water; sodium carbonate; lithium hydroxide;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether; tetrahydrofuran / 1 h / 0 °C
2: toluene / 1.17 h / 140 - 160 °C / microwave irradiation
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 0.33 h / 90 °C / microwave irradiation
4: water; lithium hydroxide / tetrahydrofuran / 48 h / 23 °C
With
water; sodium carbonate; lithium hydroxide;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; toluene;
