(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

Base Information

Chemical Name:(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide
CAS No.:1189331-82-5
Molecular Formula:C₁₈H₂₂ClNO₄S
Molecular Weight:383.896
Hs Code.:

Synonyms:(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

Suppliers and Price of (1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

Chemical Property:

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Technology Process of (1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

There total 1 articles about (1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1189331-81-4
(1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide

: 100-39-0
benzyl bromide

: 1189331-82-5
(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 23 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2009.09.019

Reference yield: 88.0%

: 1189331-82-5
(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

: 1189331-83-6
(5R)-4-benzyl-5-benzyloxymethyl-[1,3,4]-oxathiazinane-3,3-dioxide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2009.09.019

Reference yield:

: 1189331-82-5
(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

: 1189331-84-7
(5R)-4-benzyl-5-hydroxymethyl-[1,3,4]-oxathiazinane-3,3-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 80 °C

2: hydrogen / palladium / ethanol / 45 °C / 30003 Torr

With hydrogen; caesium carbonate; palladium; In ethanol; N,N-dimethyl-formamide;