(1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide

Base Information

• Chemical Name: (1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide
• CAS No.: 1189331-81-4
• Molecular Formula: C₁₁H₁₆ClNO₄S
• Molecular Weight: 293.771

Synonyms:(1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide

Chemical Property of (1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide

Chemical Property:

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Technology Process of (1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide

There total 1 articles about (1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

monochloromethanesulfonyl chloride (3518-65-8) + (2S)-2-amino-3-(benzyloxy)propan-1-ol (58577-88-1) → (1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide (1189331-81-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.09.019

Reference yield: 73.0%

(1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide (1189331-81-4) + p-Methoxybenzyl bromide (2746-25-0) → C19H24ClNO5S (1251834-17-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.09.019

Reference yield: 31.0%

(1S)-N-[(2-benzyloxy)-1-(hydroxymethyl)ethyl]chloromethane sulphonamide (1189331-81-4) + benzyl bromide (100-39-0) → (1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide (1189331-82-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 23 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.09.019

upstream raw materials:

monochloromethanesulfonyl chloride

(2S)-2-amino-3-(benzyloxy)propan-1-ol

Downstream raw materials:

(5R)-5-[(benzyloxy)methyl]-[1,3,4]-oxathiazinane-3,3-dioxide

(1S)-N-benzyl-N-[2-(benzyloxy)-1-(hydroxymethyl)ethyl]-1-chloromethane sulphonamide

C₁₉H₂₄ClNO₅S

(1S)-N-methyl-N-(1-hydroxy-3-benzyloxy-2-propyl)chloromethanesulfonamide

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