cyclohexanecarbonyl dodecanoyl peroxide

Base Information

• Chemical Name: cyclohexanecarbonyl dodecanoyl peroxide
• CAS No.: 103677-75-4
• Molecular Formula: C₁₉H₃₄O₄
• Molecular Weight: 326.477
• Mol file: 103677-75-4.mol

Synonyms:cyclohexanecarbonyl dodecanoyl peroxide

Chemical Property of cyclohexanecarbonyl dodecanoyl peroxide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of cyclohexanecarbonyl dodecanoyl peroxide

There total 2 articles about cyclohexanecarbonyl dodecanoyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

peroxylaurinoic acid (2388-12-7) + cyclohexanylcarbonyl chloride (2719-27-9) → cyclohexanecarbonyl dodecanoyl peroxide (103677-75-4)

Guidance literature:

With pyridine; In diethyl ether; at 10 ℃; for 0.5h; addition -20 deg C to -10 deg C;

DOI:10.1016/S0040-4020(01)97194-7

Reference yield:

lauric acid (143-07-7) → cyclohexanecarbonyl dodecanoyl peroxide (103677-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / 30 percent aq. H₂O₂ / H₂SO₄ / 1 h / 10 °C / addition 10 to 20 deg C

2: 90 percent / pyridine / diethyl ether / 0.5 h / 10 °C / addition -20 deg C to -10 deg C

With pyridine; dihydrogen peroxide; In diethyl ether; sulfuric acid;

DOI:10.1016/S0040-4020(01)97194-7

Reference yield:

cyclohexanecarbonyl dodecanoyl peroxide (103677-75-4) → n-Undecane (1120-21-4) + n-undecylcyclohexane (54105-66-7)

Guidance literature:

at -78 ℃; for 70h; Irradiation;

DOI:10.1016/S0040-4020(01)97194-7

upstream raw materials:

peroxylaurinoic acid

cyclohexanylcarbonyl chloride

lauric acid

Downstream raw materials:

n-Undecane

n-undecylcyclohexane