3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

Base Information

Chemical Name:3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester
CAS No.:912296-78-7
Molecular Formula:C₃₃H₃₀N₂O₇
Molecular Weight:566.61
Hs Code.:

Synonyms:3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

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Chemical Property of 3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

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Technology Process of 3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

There total 3 articles about 3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 77513-40-7
3-Benzyloxycarbonyl-phenol

: 3-benzyloxycarbonylamino-2-(2-phenyl-acetylamino)-propionic acid

: 912296-78-7
3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

Guidance literature:: With 1,1'-carbonyldiimidazole;
DOI:10.1016/j.bmc.2006.06.023

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 912296-78-7
3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: Cu(OAc)2; NaOH; MgO / H₂O / 5 h / pH 5

1.2: 49 percent / thioacetamide; AcOH / H₂O / 0.17 h / Heating

2.1: 77 percent / NaOH / H₂O / 2 h / 20 °C

3.1: 30 percent / 1,1'-carbonyldiimidazole

With sodium hydroxide; copper diacetate; magnesium oxide; 1,1'-carbonyldiimidazole; In water;
DOI:10.1016/j.bmc.2006.06.023

Reference yield:

: 103-80-0
phenylacetyl chloride

: 912296-78-7
3-(3-benzyloxycarbonylamino-2-phenylacetylamino-propionyloxy)-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaOH / H₂O / 2 h / 20 °C

2: 30 percent / 1,1'-carbonyldiimidazole

With sodium hydroxide; 1,1'-carbonyldiimidazole; In water;
DOI:10.1016/j.bmc.2006.06.023