2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione

Base Information

• Chemical Name: 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione
• CAS No.: 210366-72-6
• Molecular Formula: C₅₇H₄₇NO₄S₄
• Molecular Weight: 938.268

Synonyms:2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione

Chemical Property of 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione

Chemical Property:

Purity/Quality:

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Technology Process of 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione

There total 3 articles about 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione (210366-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / dimethylformamide / 10 h / 40 °C

2: 1.) K₂CO₃ / 1.) CH₃CN, 1 h, 2.) CH₃CN, RT, overnight

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/ja974031e

Reference yield:

potassium phtalimide (1074-82-4) → 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione (210366-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / dimethylformamide / 10 h / 40 °C

2: 1.) K₂CO₃ / 1.) CH₃CN, 1 h, 2.) CH₃CN, RT, overnight

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/ja974031e

Reference yield:

3,5-bis[(phenylsulfanyl)methyl]phenol (168414-96-8) + α,α'-dibromo-α''-phthalimidomesitylene (188257-49-0) → 2-[3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzyl]-isoindole-1,3-dione (210366-72-6)

Guidance literature:

With potassium carbonate; Yield given. Multistep reaction; 1.) CH₃CN, 1 h, 2.) CH₃CN, RT, overnight;

DOI:10.1021/ja974031e

upstream raw materials:

3,5-bis[(phenylsulfanyl)methyl]phenol

α,α'-dibromo-α''-phthalimidomesitylene

1,3,5-Tris(bromomethyl)benzene

potassium phtalimide

Downstream raw materials:

α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene

3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzylamine

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