4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

Base Information

Chemical Name:4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid
CAS No.:93330-31-5
Molecular Formula:C₁₇H₁₅ClO₃
Molecular Weight:302.757
Hs Code.:

Synonyms:4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

Suppliers and Price of 4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

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Technology Process of 4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

There total 7 articles about 4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32383-67-8,83072-25-7,32383-66-7
(E)-2,3-bis(4-methoxyphenyl)acrylic acid

: 93330-31-5
4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

Guidance literature:: With thionyl chloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm0498708

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 93330-31-5
4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine; acetic anhydride / 12 h / 140 °C

2: SOCl₂ / CH₂Cl₂; dimethylformamide / 1 h / 20 °C

With thionyl chloride; acetic anhydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0498708

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 93330-31-5
4-Methoxy-α-<4-methoxy-phenyl>-trans-zimtsaeurechlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine; acetic anhydride / 12 h / 140 °C

2: SOCl₂ / CH₂Cl₂; dimethylformamide / 1 h / 20 °C

With thionyl chloride; acetic anhydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0498708