radical anion of chloranil

Base Information

• Chemical Name: radical anion of chloranil
• CAS No.: 7646-32-4
• Molecular Formula: C₆Cl₄O₂*Na
• Molecular Weight: 291.856

Synonyms:radical anion of chloranil

Chemical Property of radical anion of chloranil

Chemical Property:

Purity/Quality:

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Technology Process of radical anion of chloranil

There total 2 articles about radical anion of chloranil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium N,N-diethyldithiocarbamate (148-18-5) + chloranil (118-75-2) → bis-ethoxythiocarbonyldisulfane (502-55-6) + diethyldithiocarbamate radical (54451-16-0) + radical anion of chloranil (7646-32-4) + C6Cl4O2(2-)*2Na(1+) (7646-32-4)

Guidance literature:

In acetone; at 20 ℃; Product distribution; reactants ratio dependence, ESR monitoring; also with ethyl potassium xanthate;

DOI:10.1007/BF00961114

Reference yield:

sodium N,N-diethyldithiocarbamate (148-18-5) + chloranil (118-75-2) → bis-ethoxythiocarbonyldisulfane (502-55-6) + diethyldithiocarbamate radical (54451-16-0) + radical anion of chloranil (7646-32-4) + C6Cl4O2(2-)*2Na(1+) (7646-32-4)

Guidance literature:

In acetone; at 20 ℃; Product distribution; reactants ratio dependence, ESR monitoring; also with ethyl potassium xanthate;

DOI:10.1007/BF00961114

Reference yield:

15-crown-5 (33100-27-5) + radical anion of chloranil (7646-32-4) → C6Cl4O2(1-)*C20H40KO10(1+)

Guidance literature:

In dichloromethane; Inert atmosphere;

DOI:10.1039/b811816g

upstream raw materials:

sodium N,N-diethyldithiocarbamate

chloranil

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