bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

Base Information

Chemical Name:bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate
CAS No.:1041482-22-7
Molecular Formula:C₂₈H₃₇N₃O₄
Molecular Weight:479.619
Hs Code.:

Synonyms:bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

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Chemical Property of bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

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Technology Process of bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

There total 5 articles about bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 53001-06-2
2,2-diphenyl-4-pentenylamine

: 207857-15-6
1,3-di(tert-butyloxycarbonyl)-2-(trifluoromethylsulfonyl)guanidine

: 1041482-22-7
bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403891

Reference yield:

: 332882-82-3,154476-57-0
1,3-bis(t-butoxycarbonyl)guanidine

: 1041482-22-7
bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With triethylamine; In dichloromethane;
DOI:10.1002/chem.201403891

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1041482-22-7
bis-tert-butyl (2,2-diphenylpent-4-en-1-yl)amino-methylylidenebiscarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide; sodium carbonate / dimethyl sulfoxide / 0.08 h / Inert atmosphere; Schlenk technique

1.2: 60 h / 40 °C / Inert atmosphere; Schlenk technique

2.1: triethylamine / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

3.1: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With sodium carbonate; triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/chem.201403891