methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

Base Information

Chemical Name:methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate
CAS No.:1001017-53-3
Molecular Formula:C₂₂H₃₀N₆O₄
Molecular Weight:442.518
Hs Code.:

Synonyms:methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

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Chemical Property of methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

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Technology Process of methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

There total 1 articles about methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1001017-52-2
[4-({[3-(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetic acid

: 1001017-53-3
methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

Guidance literature:: methanol; [4-({[3-(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetic acid; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 24h;

With water; sodium hydrogencarbonate; In 1,4-dioxane; methanol; pH=8;

Reference yield:

: 1001017-53-3
methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

: 60853-81-8
N,N-dimethylaminoacetyl chloride hydrochloride

: methyl (4-{[[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](N,N-dimethylglycyl)amino]methyl}phenyl)acetate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 10h;

Reference yield:

: 1001017-53-3
methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate

: 37784-17-1,59433-50-0
N-(tert-butoxycarbonyl)-D-proline

: [2R]-(4-{[[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-purin-9-yl)propyl]-(pyrrolidine-2-carbonyl)-amino]-methyl}-phenyl)-acetic acid methyl ester

Guidance literature:: methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]amino}methyl)phenyl]acetate; N-(tert-butoxycarbonyl)-D-proline; With HATU; In dichloromethane; at 20 ℃; for 17h;

With trifluoroacetic acid; In dichloromethane; for 4h;