C₁₄H₁₇BrO

Base Information

• Chemical Name: C₁₄H₁₇BrO
• CAS No.: 1211936-74-1
• Molecular Formula: C₁₄H₁₇BrO
• Molecular Weight: 281.192

Synonyms:C₁₄H₁₇BrO

Chemical Property of C₁₄H₁₇BrO

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₇BrO

There total 1 articles about C₁₄H₁₇BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H18O2 (1211936-64-9) → C14H17BrO (1211936-74-1)

Guidance literature:

With phosphorus tribromide; In diethyl ether; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/anie.200904527

Reference yield: 74.0%

C14H17BrO (1211936-74-1) + ethyl acetate (141-78-6) → C18H24O3 (1211936-65-0)

Guidance literature:

ethyl acetate; With copper(I) bromide dimethylsulfide complex; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.533333h; Inert atmosphere;

C₁₄H₁₇BrO; In tetrahydrofuran; at -78 ℃; for 0.833333h; Inert atmosphere;

DOI:10.1002/anie.200904527

Reference yield: 57.0%

propanoic acid methyl ester (554-12-1) + C14H17BrO (1211936-74-1) → C18H24O3 (1211936-75-2)

Guidance literature:

propanoic acid methyl ester; With copper(I) bromide dimethylsulfide complex; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.533333h; Inert atmosphere;

C₁₄H₁₇BrO; In tetrahydrofuran; at -78 ℃; for 0.833333h; Inert atmosphere;

DOI:10.1002/anie.200904527

upstream raw materials:

C₁₄H₁₈O₂

Downstream raw materials:

C₁₈H₂₄O₃

C₁₈H₂₄O₃

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