(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

Base Information

Chemical Name:(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate
CAS No.:951171-17-8
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

Synonyms:(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

Chemical Property:

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Technology Process of (E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

There total 2 articles about (E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 80704-08-1
(E)-[5,5-dimethyl-6-(3-oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

: 951171-17-8
(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

Guidance literature:: With acetic anhydride; t-butyl chromate; In tert-butyl alcohol; for 2h; Heating;
DOI:10.1016/j.bmcl.2007.06.018

Reference yield:

: 127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7
alpha-ionone

: 951171-17-8
(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / iodine / benzene / 2.5 h / 100 °C

2: 10 percent / t-butyl alcohol; acetic anhydride; CrO₃ / 2 h / Heating

With chromium(VI) oxide; iodine; acetic anhydride; tert-butyl alcohol; In benzene;
DOI:10.1016/j.bmcl.2007.06.018

Reference yield: 65.0%

: 951171-17-8
(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate

: 88738-78-7
bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate

: 951171-19-0
C₁₈H₂₄O₆

Guidance literature:: bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 1h;

(E)-[6-hydroxy-5,5-dimethyl-3-oxo-6-(oxobut-1-enyl)cyclohex-1-enyl]methyl acetate; In tetrahydrofuran; toluene; at 20 ℃; for 18h; Further stages.;
DOI:10.1016/j.bmcl.2007.06.018