(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

Base Information

Chemical Name:(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde
CAS No.:1070226-17-3
Molecular Formula:C₁₁H₁₂O
Molecular Weight:160.216
Hs Code.:

Synonyms:(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

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Technology Process of (1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

There total 9 articles about (1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 175519-56-9
(1S,2S)-1-hydroxymethyl-2-methyl-2-phenylcyclopropane

: 1070226-17-3
(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2008.08.061

Reference yield:

: 201230-82-2
carbon monoxide

: 65051-83-4
3-methyl-3-phenylcyclopropene

: 1070226-17-3
(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

: 1070226-20-8
C₁₁H₁₂O

Guidance literature:: With R-(-)-1,13-bis(diphenylphosphino)-7,8-dihydro-6H-dibenzo[f,h][1,5]dioxonin; Rh(acac)2(CO)2; hydrogen; In toluene; at 60 ℃; for 18h; under 7757.43 Torr; optical yield given as %ee; Inert atmosphere; Autoclave;
DOI:10.1021/ja805059f

Reference yield:

: 201230-82-2
carbon monoxide

: 65051-83-4
3-methyl-3-phenylcyclopropene

: 1070226-17-3
(1S,2S)-2-methyl-2-phenylcyclopropanecarbaldehyde

: C₁₁H₁₂O

: C₁₁H₁₂O

: 1070226-20-8
C₁₁H₁₂O

Guidance literature:: With Rh(acac)2(CO)2; Josiphos SL-J₀₀₂-1; hydrogen; In toluene; at 60 ℃; under 7757.43 Torr; optical yield given as %ee; Inert atmosphere; Autoclave;
DOI:10.1021/ja805059f