5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene
CAS No.:1380075-76-2
Molecular Formula:C₂₆H₂₆BrNO₄
Molecular Weight:496.401
Hs Code.:

Synonyms:5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

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Technology Process of 5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

There total 5 articles about 5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1380075-75-1
2-bromo-4-nitro-5,6,7,8-tetrahydronaphthalen-1-ol

: bis(4-benzyloxy-3-isopropylphenyl)iodonium tetrafluoroborate

: 1380075-76-2
5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With bronze powder; triethylamine; In dichloromethane; at 20 ℃; for 120h;
DOI:10.1016/j.bmc.2012.03.056

Reference yield:

: 1-benzyloxy-2-isopropylbenzene

: 1380075-76-2
5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine tris(trifluoroacetate); acetic anhydride; trifluoroacetic acid / 16 h / 4 °C

1.2: 0.5 h

2.1: bronze powder; triethylamine / dichloromethane / 120 h / 20 °C

With bronze powder; iodine tris(trifluoroacetate); acetic anhydride; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2012.03.056

Reference yield:

: 100-39-0
benzyl bromide

: 1380075-76-2
5-(4-benzyloxy-3-isopropylphenoxy)-6-bromo-8-nitro-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 29 h / Reflux

2.1: iodine tris(trifluoroacetate); acetic anhydride; trifluoroacetic acid / 16 h / 4 °C

2.2: 0.5 h

3.1: bronze powder; triethylamine / dichloromethane / 120 h / 20 °C

With bronze powder; iodine tris(trifluoroacetate); acetic anhydride; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2012.03.056