Benzoyl chloride, 3-methoxy-4-methyl- (9CI)

Base Information

• Chemical Name: Benzoyl chloride, 3-methoxy-4-methyl- (9CI)
• CAS No.: 87808-44-4
• Molecular Formula: C9H9 Cl O2
• Molecular Weight: 184.622
• Hs Code.: 2918990090
• Mol file: 87808-44-4.mol

Synonyms:3-Methoxy-4-methylbenzoylchloride; 4-Methyl-3-methoxybenzoyl chloride

Chemical Property of Benzoyl chloride, 3-methoxy-4-methyl- (9CI)

Chemical Property:

• PSA: 26.30000
• LogP: 2.38260

Purity/Quality:

99%, ^*data from raw suppliers

3-Methoxy-4-methylbenzoyl chloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoyl chloride, 3-methoxy-4-methyl- (9CI)

There total 1 articles about Benzoyl chloride, 3-methoxy-4-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-p-toluic acid (7151-68-0) → 3-methoxy-4-methylbenzoyl chloride (87808-44-4)

Guidance literature:

With thionyl chloride;

DOI:10.1002/hlca.19360190158

Reference yield: 100.0%

3-methoxy-4-methylbenzoyl chloride (87808-44-4) + 2-amino-phenol (95-55-6) → N-(2-hydroxyphenyl)-3-methoxy-4-methylbenzamide (669091-09-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2003.10.021

Reference yield: 100.0%

6-methoxybenzothiazol-2-ylamine (1747-60-0) + 3-methoxy-4-methylbenzoyl chloride (87808-44-4) → 3-methoxy-4-methyl-N-(6-methoxy-1,3-benzothiazol-2-yl)benzamide (1361253-21-5)

Guidance literature:

With pyridine; for 4h; Reflux;

DOI:10.1021/jm201711b

upstream raw materials:

3-methoxy-p-toluic acid

Downstream raw materials:

N-(2-hydroxyphenyl)-3-methoxy-4-methylbenzamide

5-bromo-2-methylphenol methyl ether

3-methoxy-4-methylbenzaldehyde

(3-methoxy-4-methylphenyl)[5-(4-methoxyphenyl)-2-thienyl]methanone