Technology Process of C33H44O5Si
There total 9 articles about C33H44O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chromium dichloride;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
stereoselective reaction;
Inert atmosphere;
DOI:10.1002/chem.201002380
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.5 h / -50 °C / Inert atmosphere
2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Inert atmosphere; Molecular sieve
2.2: 1.5 h / 20 °C / Inert atmosphere
3.1: dicyclohexylmethylamine; tetrabutylammomium bromide; palladium diacetate / N,N-dimethyl-formamide / 1 h / 140 °C
4.1: hydrogenchloride / methanol / 4 h / 0 - 20 °C / Inert atmosphere
5.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere
6.1: chromium dichloride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
With
chromium dichloride; hydrogenchloride; tetrapropylammonium perruthennate; dicyclohexylmethylamine; tetrabutylammomium bromide; palladium diacetate; Dess-Martin periodane; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
2.2: Takai olefination / 3.1: Heck cross-coupling / 6.1: Takai reaction;
DOI:10.1002/chem.201002380
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrazine hydrate / 0 - 20 °C
1.2: 0.17 h / 20 °C / Inert atmosphere
2.1: chromium dichloride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
With
chromium dichloride; hydrazine hydrate;
In
tetrahydrofuran;
2.1: Takai reaction;
DOI:10.1002/chem.201002380
