benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

Base Information

Chemical Name:benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside
CAS No.:137232-61-2
Molecular Formula:C₅₂H₄₄O₁₄
Molecular Weight:892.913
Hs Code.:

Synonyms:benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

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Chemical Property of benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

Chemical Property:

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Technology Process of benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

There total 5 articles about benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2
D-Xylose

: 137232-61-2
benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / acetyl chloride / 24 h / 45 °C

2: 1.) dibutyltin oxide / 1.) benzene, reflux, overnight, 2.) 0 deg C

3: 91 percent / collidine, molecular sieves / silver triflate / CH₂Cl₂ / 0.25 h / 0 °C

With 2,3,5-trimethyl-pyridine; molecular sieve; di(n-butyl)tin oxide; acetyl chloride; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jo00025a013

Reference yield:

: 98-88-4
benzoyl chloride

: 137232-61-2
benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide / 1.) benzene, reflux, overnight, 2.) 0 deg C

2: 91 percent / collidine, molecular sieves / silver triflate / CH₂Cl₂ / 0.25 h / 0 °C

With 2,3,5-trimethyl-pyridine; molecular sieve; di(n-butyl)tin oxide; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jo00025a013

Reference yield:

: 18403-12-8
benzyl β-D-xylopyranoside

: 137232-61-2
benzyl (2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-(1<*>3)-2,4-di-O-benzoyl-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide / 1.) benzene, reflux, overnight, 2.) 0 deg C

2: 91 percent / collidine, molecular sieves / silver triflate / CH₂Cl₂ / 0.25 h / 0 °C

With 2,3,5-trimethyl-pyridine; molecular sieve; di(n-butyl)tin oxide; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jo00025a013