tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

Base Information

Chemical Name:tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate
CAS No.:1217258-84-8
Molecular Formula:C₃₂H₃₂N₂O₅
Molecular Weight:524.616
Hs Code.:

Synonyms:tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

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Chemical Property of tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

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Technology Process of tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

There total 3 articles about tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3-phenyl-allylideneamino)-acetic acid tert-butyl ester

: 198021-41-9
[(4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl]acetyl chloride

: 1217258-84-8
tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

Guidance literature:: [(4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl]acetyl chloride; With triethylamine; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

(3-phenyl-allylideneamino)-acetic acid tert-butyl ester; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

Reference yield:

: 1020096-34-7
C₁₅H₁₉NO₂

: 198021-38-4
[(4S,5R)-4,5-diphenyloxazolidin-2-on-3-yl]acetic acid

: 1217258-84-8
tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

Guidance literature:: [(4S,5R)-4,5-diphenyloxazolidin-2-on-3-yl]acetic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1.5h;

C₁₅H₁₉NO₂; With triethylamine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

Reference yield:

: 1020096-34-7
C₁₅H₁₉NO₂

: 198021-41-9
[(4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl]acetyl chloride

: 1217258-84-8
tert-butyl-2-((3S,4R)-2-oxo-3-((4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl)-4-((E)-styryl)azetidin-1-yl)acetate

Guidance literature:: [(4S,5R)-2-oxo-4,5-diphenyloxazolidin-3-yl]acetyl chloride; With triethylamine; In dichloromethane; at -78 ℃; for 0.333333h;

C₁₅H₁₉NO₂; In dichloromethane; at -78 - 0 ℃; for 2h;