dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

Base Information

Chemical Name:dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron
CAS No.:103816-90-6
Molecular Formula:C₂₉H₂₉FeO₆P
Molecular Weight:560.366
Hs Code.:

Synonyms:dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

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Chemical Property of dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

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Technology Process of dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

There total 1 articles about dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 103816-89-3
dicarbonyl[methyl(2-5-η-cyclohepta-2,4-dienyl)acetate](triphenyl phosphite)iron

: 1191-15-7
diisobutylaluminium hydride

: 103816-90-6
dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

Guidance literature:: In tetrahydrofuran; hexane; addn. hexane soln. of Al-compd. to THF soln. of Fe-compd. (-78°C), stirring, (-78°C, 4 h); warming to room temp. (overnight), addn. of water, stirring (30 min), addn. of Et2O, filtration (Celite), washing (water), drying (MgSO4), filtration, solvent removal, preparative TLC;;

Reference yield: 90.0%

: 1313-13-9
manganese(IV) oxide

: 103816-90-6
dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

: 103816-95-1
Fe(CO)2(P(OC₆H₅)3)(C₇H₈(CH₂CH₂O))

Guidance literature:: In benzene; refluxing MnO2 (overnight, water separator), cooling, addn. Fe-compd., refluxing (20 min); cooling, filtration (Celite), removal solvent;

Reference yield: 79.0%

: 103816-90-6
dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

: 108-24-7
acetic anhydride

: 103816-92-8
dicarbonyl[1-4-η-5-(2-acetoxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron

Guidance literature:: With water; In pyridine; stirring (room temp., 23 h), addn. of H2O, stirring (30 min); extn. (Et2O), washing (dil. HCl), drying (MgSO4), filtration, solvent removal, chromy.; elem. anal.;