2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl

Base Information

Chemical Name:2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl
CAS No.:392292-92-1
Molecular Formula:C₃₄H₄₆CoN₃
Molecular Weight:555.753
Hs Code.:

Synonyms:2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl

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Chemical Property of 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl

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Technology Process of 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl

There total 5 articles about 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 308359-86-6,207129-97-3
2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine cobalt(II) dichloride

: 917-54-4
methyllithium

: 392292-92-1
2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridinecobaltmethyl

Guidance literature:: In diethyl ether; (Ar); a soln. of Co complex cooled to -78°C, CH3Li in ether addeddropwise, allowed to warm to room temp.; filtered, evapd. (vac.);
DOI:10.1021/ja052129k

Reference yield: 81.0%

: 308359-86-6,207129-97-3
2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine cobalt(II) dichloride

: 75-16-1
methylmagnesium bromide

: 392292-92-1
[CoMe(2,6-(MeCN(2,6-(CHMe₂)2C₆H₃))2C₅H₃N)]

Guidance literature:: In diethyl ether; (N2); using Schlenk techniques; treatment dropwise of suspn. of CoCl2(C5H3N(C(Me)NC6H3(CHMe2)2)2) in Et2O at -78°C with soln. of MeMgBr (2 equiv.) in Et2O; warming to ambient temp., stirring for 24 h at room temp.; removal of volatiles under reduced pressure, extn. with toluene, filtration, removal of volatiles under reduced pressure, elem. anal.;
DOI:10.1021/om049032b

Reference yield:

: 308359-86-6,207129-97-3
2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine cobalt(II) dichloride

: 392292-92-1
[CoMe(2,6-(MeCN(2,6-(CHMe₂)2C₆H₃))2C₅H₃N)]

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃Li / toluene

2: diethyl ether

With CH₃Li; In diethyl ether; toluene;
DOI:10.1002/1521-3773(20011217)40:24<4719::AID-ANIE4719>3.0.CO;2-O