1H-Benzimidazole,2-(2-furanyl)-5-methyl-(9CI)

Base Information

• Chemical Name: 1H-Benzimidazole,2-(2-furanyl)-5-methyl-(9CI)
• CAS No.: 83330-28-3
• Molecular Formula: C₁₂H₁₀N₂O
• Molecular Weight: 198.224
• Hs Code.: 2934999090
• Mol file: 83330-28-3.mol

Synonyms:1H-Benzimidazole,2-(2-furanyl)-5-methyl- (9CI); Benzimidazole, 2-(2-furyl)-5(or 6)-methyl- (7CI)

Chemical Property of 1H-Benzimidazole,2-(2-furanyl)-5-methyl-(9CI)

Chemical Property:

• PSA: 41.82000
• LogP: 3.13130

Purity/Quality:

2-(furan-2-yl)-5-methyl-1H-benzimidazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Benzimidazole,2-(2-furanyl)-5-methyl-(9CI)

There total 4 articles about 1H-Benzimidazole,2-(2-furanyl)-5-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

(2-furyl)methyl alcohol (98-00-0,25212-86-6,93793-62-5) + 4-methyl-2-nitroaniline (89-62-3) → 2-(furan-2-yl)-6-methyl-1H-benzo[d]imidazole (83330-28-3)

Guidance literature:

With cobalt acetylacetonate; sodium t-butanolate; In 1,4-dioxane; at 135 ℃; for 24h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.joc.9b02090

Reference yield:

3-amino-4-(2-furoylamino)toluene (79324-94-0) → 2-(furan-2-yl)-6-methyl-1H-benzo[d]imidazole (83330-28-3)

Guidance literature:

With acetic acid; In water; dimethyl sulfoxide; Inert atmosphere; Heating;

DOI:10.1021/jo9017183

Reference yield:

furfural (98-01-1) + 4-methyl-1,2-diaminobenzene (496-72-0) → 2-(furan-2-yl)-6-methyl-1H-benzo[d]imidazole (83330-28-3)

Guidance literature:

With copper diacetate; In methanol; water;

DOI:10.1021/jo01053a063

upstream raw materials:

furfural

4-methyl-1,2-diaminobenzene

furan-2-carboxylic acid ethyl imino ester

3-amino-4-(2-furoylamino)toluene

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